Archive for March, 2007

Social Explanatory Style as a Foundation of Empathic Orientation

We examined whether peoples social explanations the explanatory frameworks they use to make sense of others behaviors and outcomes are tied to their social orientation, or the extent to which they demonstrate tendencies such as empathy and forgiveness. While evidence for a social explanatory style (i.e., a characteristic manner of explaining behavior across targets and contexts) was mixed, results demonstrated that social explanations interacted with epistemic motives (e.g., attributional complexity) to predict social orientation.

Saturday, March 24th, 2007 Psychology Comments Off

Surface Characterization of a Synergistic Pt-Rh/gamma-Al2O3 Catalyst Through NO Adsorption

Effective bimetallic catalysts often exhibit synergy. Synergy is defined as the bimetallic catalyst being more active and/or selective than either of its constituent metals. The activity and selectivity of bimetallic catalysts is dependent upon their particle surface compositions which in turn is a function of individual particle composition, pretreatment conditions, and other factors. This study compares the activity and surface composition of a Pt(95%)-Rh(5%)/gamma-Al2O3 catalyst (95/5) to Pt/gamma-Al2O3, Rh/gamma-Al2O3, and gamma-Al2O3. Reacting NO and H2 over each of the catalysts resulted in the following order of relative NO reduction activity 95/5 > Pt/gamma-Al2O3 > Rh/gamma-Al2O3 >> Al2O3. The maximum synergistic performance of 95/5, a five-fold increase over the activity of Pt/gamma-Al2O3, was obtained after conditioning the catalyst by reacting it at 250oC for 10 h, and the synergistic performance of 95/5 was unaffected by a 24 h reduction at 300oC. The surface composition of the prepared catalysts was investigated with in-situ FTIR spectroscopy at 100oC, 150oC and 200oC using NO as a probe molecule. The obtained spectra indicate that both Pt and Rh are present on the surface of the synergistic 95/5 catalyst. The amount of Rh on the catalyst surface increased as a function of NO adsorption temperature. Rh present on the surface of the alloy nanoparticles was in a reduced state at 150oC and 200oC, while on a monometallic Rh/gamma-Al2O3 catalyst some of Rh present was partially oxidized. Analytical electron microscopy has been used to show that the metals on the surface of synergistic Pt-Rh bimetallics exist as a single phase of Pt-rich Pt-Rh alloy nanoparticles, while both Pt-rich and Rh-rich alloy phases are present on non-synergistic Pt-Rh bimetallics.

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Wednesday, March 21st, 2007 Chemical Engineering, Materials Science & Engineering Comments Off

Solvation Controlled Luminescence of Sm(II) Complexes

Changes in solvation of samarium diiodide (SmI2) can significantly alter the interaction between a ligand and metal. Addition of the appropriate crown ether to SmI2 in acetonitrile not only stabilizes the ground state complex but also generates a highly luminescent complex. The advantage of direct excitation of lanthanide(II) complexes includes elimination of different deactivation pathways as well as the multi-step syntheses involved in preparing antenna ligands necessary for producing luminescent lanthanide(III) complexes. We demonstrate how controlling the coordination sphere of SmI2 through changes in solvation induces remarkable changes both in the ground and excited states. By providing a chelating ligand for SmI2 in a solvent incapable of displacing it significantly enhances the luminescent properties of Sm(II) by: 1.) encapsulating the metal through a strong metal-ligand interaction and 2) decreasing the frequency of solvent collision. This study led to the discovery of the longest reported excited-state lifetime for a Sm(II) complex in solution.

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Friday, March 16th, 2007 Chemistry Comments Off

Role of Reactive Surfactants in Miniemulsion Polymerization

Reactive surfactants show a promising approach to reduce the negative effects where by the surfactant is chemically incorporated into the latex particles during the course of the polymerization so that desorption of the surfactant from the latex or migration in the resulting polymer film is impeded. One of its main characteristics is that reactive surfactant should be incorporated onto the polymer particles surfaces at the very end of the reaction process .Miniemulsion polymerization is therefore proposed as an alternative process to increase the amount of the surfactant incorporated on the particle surfaces and to minimize the amount of the buried surfactant since miniemulsion polymerize primarily via droplet nucleation mechanism. › Continue reading

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Wednesday, March 7th, 2007 Chemical Engineering Comments Off

Reversible Self-Assembly of Hydrophilic Inorganic Polyelectrolytes into Highly Conservative, Vesicle-like Structures

The hydrophilic polyoxometalate (POM) macroanions are inorganic polyelectrolytes which offer a direct connection between simple ions and organic polyelectrolytes. POM solutions are perfect model systems for studying polyelectrolyte solutions because they are identical in size, shape, mass and charges, with easily tunable charge density.

Many types of POM macroanions are highly soluble but undergo reversible self-assembly to form uniform, stable, soft, single-layer vesicle-like blackberry structures containing >1000 individual POMs in dilute solutions. The driving force of the blackberry formation is likely counterion-mediated attraction (like-charge attraction). The blackberry size can be accurately controlled by solvent quality, or the charge density on macroions. Many unexpected phenomena have been observed in these novel systems. Blackberry structures may be analogous to virus shell structures formed by capsid proteins.

References:
Nature, 2003, 426, 59; JACS, 2002, 124, 10942; 2003, 125, 312; 2004, 126, 16690; 2005, 127, 6942; 2006, 128, 10103.

Tuesday, March 6th, 2007 Chemistry Comments Off